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以水为反应介质,采用碳酸钠为缚酸剂,在微波辐射的条件下,使芳胺与σ-溴代苯乙酮反应,合成N,N-二烷基化苯胺。其中,探讨了微波功率、缚酸剂种类和缚酸剂剂量等因素对反应产率的影响。该方法具有环境友好、后处理简便、反应时间短和产率高等优点[1,2]。
微波辐射下水相合成N,N-二烷基化芳胺
【摘 要】
：
以水为反应介质,采用碳酸钠为缚酸剂,在微波辐射的条件下,使芳胺与σ-溴代苯乙酮反应,合成N,N-二烷基化苯胺。其中,探讨了微波功率、缚酸剂种类和缚酸剂剂量等因素对反应产率的影响。该方法具有环境友好、后处理简便、反应时间短和产率高等优点[1,2]。
【机 构】
：
石家庄学院,河北省石家庄市开发区长江大道6号,050035 河北中医学院,河北省石家庄市中山东路3
【出 处】
：
中国化学会第29届学术年会
【发表日期】
：
2014年1期
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