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A series of well-defined amphiphilic graft copolymers,consisting of a hydrophilic poly(2-hydroxyethyl acrylate) (PHEA) backbone and hydrophobic polystyrene side chains,was synthesized by the combination of reversible addition-fragmentation chain transfer (RAFT) polymerization,atom transfer radical polymerization (ATRP),and the grafting-from strategy.