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A series of 4″-substituted 4′-phenyl-2,2′:6′,2″-terpyridine compounds,bearing hydrogen(1),methoxyl(2),methylsulfonyl(3),cyano(4),methyl(5),phenyl(6),iodo(7),or p-methyl-phenyl(8) were synthesized and characterized by IR,elemental analysis,1H NMR,13C NMR and X-ray determination.