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Our research focuses on the oxidative coupling to develop a novel and efficient bond-formation method betweentwo nucleophiles.We have successfully developed three generations of oxidative coupling.In addition,in-depthunderstanding toward the reactions is the other focus.Recently,a new series of oxidative coupling reactions have beendeveloped.New insights into the reaction mechanism have also been revealed by operando X-ray absorption,Raman,electron paramagnetic resonance,and nuclear magnetic resonance spectroscopy.