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Application of different approach for resection of skull base tumor
【机 构】
：
Department of Oral and Maxillofacial Surgery,the Affiliated Stomatological Hospital of Xingjian Uygu
【出 处】
：
12th International Congress on Oral Cancer & 24th Congress o
【发表日期】
：
2008年12期
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目的：本研究采用超高效液相色谱-电喷雾四极杆串联质谱同时测定猪肝中的阿维菌素和伊维菌素,并对提取溶剂、净化方法以及测定技术进行探讨.方法：猪肝样品均质后用乙腈提取,碱性氧化铝固相萃取柱(SPE)净化,采用串联质谱电喷雾电离ESI(+),多反应监测模式(MRM)检测,以保留时间和子离子比定性,外标法定量.结果：方法检出限(LOD)均为2.0μg/kg,定量限(LOQ)为5.0μg/L,两种药物的线性
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