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The critical issue to enhancing the stored energy densities lies in the development of new Li-ion battery technology is the achievement of advanced storage lithium materials.Intensive studies have been focused on enhancing the performance and reducing the cost of Sn-based anode materials for the high capacity.In present work, the approach of chemical reduction method was employed to prepare the nano-sized Sn2SbNi alloy composites used as anode material for rechargeable lithium ion batteries.