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A novel heterobimetallic 2-dimensional layer complex,[FeⅢ(bpy)(CN)4]2MnⅡ2·2H2O [bpy=2,2-bipyridine](1)has been prepared by diffusing and its structure determined by single crystal X-ray diffraction.This complex is made of neutral bimetallic [FeⅢ(bpy)(CN)4]2MnⅡ2 layers and uncoordinated water molecules located between the layers.