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The reaction of 2-hydroxy-1,2-di(pyridin-2-yl)ethanone,NH4OAC,and CuBr2 in EtOH gave a coordination polymer of composition [CuBrL](2),where the ligand L(L = 2,3,5,6-tetra(pyridin-2-yl)piperazine)was generated by metal-mediated solverthermal in situ metal-ligand reaction.