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Due to the low surface energy, the fluoride compoums could migrated to the surface in a blending solutions.[1-2] For the preparation of photo-sensitive nanofibers, a fluorinated aliphatic chain of diphenyl ketone photoinitiator EBPFOA was synthesized and characterized.The PAN and EBPFOA blending solution with DMF as the solvent was electrospun to prepare photo-sensitive nanofibers.