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Lanthanum Molybdenum Oxide were synthesized by solid state reaction in air.The resulting Lanthanum Molybdenum Oxide were systematically characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM),and the catalytic activity of Lanthanum Molybdenum Oxide were investigated in I3-/I-electrolyte by electrochemical and photoelectrochemical methods.