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A novel Fibre-Metal Laminates (FMLs) based on carbon fibre reinforced PMR polyimide were prepared using a hot press process in this paper.Pre-treatment on the titanium surface were conducted prior to laminating.Scanning Electron Microscope (SEM) were used to observe the morphologies of the titanium and the cross-sections of the FMLs.SEM results showed that micro-roughness structures were formed on the titanium surface after anodization.