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A simple and reliable electrochemical method for the quantitative determination of catechol (CC) was developed on Au-TiO2 nanocomposite modified gold electrode.The modified electrode exhibited excellent electrochemical activity and reversibility towards the oxidation of catechol in 0.1M phosphate buffer solution (PBS, pH7.0).The electrochemical response dependences of the modified electrode on pH of solution and the applied potential were studied.