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Reactive sorption enhanced reforming process ( ReSER) is an efficient hydrogen production technology based on a combine of the catalytic reforming reaction and CO2 separation on a sorption complex catalyst of Ni-CaO/Al2O3.In this study,we prepared a Ni@SiO2-CaO/Al2O3 catalyst via micro-scale hydrolysis of Si(OC2H5)4 to form SiO2 layer on the nano Ni(OH)2 colloidal particles in an adsorption phase.