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In this work,two types of new amination polychloromethyl styrene nanolatex and coated capillary column were successfully prepared.They are methyldiethanolamine amination polychloromethyl styrene nanolatex coated capillary column(ccc-MDEAPL) and dimethylethanolamine aminated polychloromethyl styrene nanolatex coated capillary column(ccc-DMEAPL).