【摘 要】
：
Using 1,4,7,10,13,16-Hexaoxacyclooctadecane as phase transfer catalyst, N,N-Diethylaniline is synthesized by reaction of aniline with bromoethane under atmo
【机 构】
：
Department of Enuironmental Science and Chemical Engineering, Dalian Jiaotong University, Liaoning,
【出 处】
：
2010中国可再生能源科技发展大会
论文部分内容阅读
Using 1,4,7,10,13,16-Hexaoxacyclooctadecane as phase transfer catalyst, N,N-Diethylaniline is synthesized by reaction of aniline with bromoethane under atmospheric pressure.The factors affecting the yield of the target product have been studied.The optimal reaction conditions are molar ratio of aniline to bromoethane, 1:1.50;35× 10-2 sodium hydroxide solution, 45ml;catalyst, 0.8g;reaction temperature, 55℃;reaction time, 4h;under normal atmosphere.The yield of N,N-diethylaniline is 73.1%.
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