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A three-dimensional(3D)metal-organic frameworks(MOFs),namely,[Yb3(μ3-O)3-(μ2-O)(DDLA)2.5(2,2'-BIPY)](1)(2,2-dipyridyl-4,4-dicarboxylic acid = H2DDLA,2,2'-BIPY = 2,2'-bipyridine),has been synthesized via solvent-thermal method.