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A new Diels-Alder Adduct of C60 with 1,1-biindene (CB) has been synthesized.The Langmuir trough study of this new fullerene derivative indicates that floating film could form monomolecular thick film at the air/water interface at lower concentration, and can be well transferred the floating mixed CB and arachidic acid film onto substrates using the Langmuir-Blodgett (LB) technique.