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Because of its high surface areas, tunable pore sizes, and periodic pore arrangements, mesoporous cobalt ferrite has been widely used in many areas, such as magnetic sensors, message recording, etc.There have been many strategies to synthesize ordered mesoporous metal materials, however, mesoporous CoFe2O4 prepared by "two-solvent" route isnt reported yet.Based on the nanocasting strategy, highly ordered mesoporous CoFe2O4 was synthesized via "two-solvent" impregnation method with SBA-15 as the template.