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It has been proposal that kinetically stabilized of nano-materials should be developed to nano/micro hierarchical structures;this strategy can take both the advantages of nano-sized building blocks and micro-sized assemblies.Recently, multi-shelled hematite hollow sphere were synthesized by using carbonaceous microspheres as the sacrificial templates.Duo to the hydrophilic of the carbonaceous microspheres and mesoporosity property.The thickness and the number of shells and shell structure can be accurately controlled by adjusting the precursor concentration and diffusion media surface tension.