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Manganese substituted goethite(α-FeOOH)was designed in the atomic scale by hydrothermal co-precipitation with Fe(NO3)3 and Mn(NO3)2 as the metal precursors.Characterization results of XRD,FTIR,XPS,SEM,EDS and HRTEM showed that manganese was successfully incorporated into the structure of α-FeOOH.