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Photoionization mass spectrometry(PIMS)as a powerful method has been widely utilized and provided valuable insight in the field of gas-phase reactions.In this talk we will present a home-made vacuum ultraviolet(VUV)photoionizationorthogonal time-of-flight mass spectrometer(TOFMS)coupled with a microwave discharge generator and a fast flow tube reactor to study radical reactions of atmospheric and combustion interests.