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In the present work, capric acid (CA) and lauric acid (LA) were selected to prepare binary CA-LA eutectic by melt-blending, and then the composite nanofibers of capric-lauric acid/polyethylene terephthalate (CA-LA/PET) in which CA-LA acts as solid-liquid phase change material (PCM) and PET acts as a supporting matrix, were successfully fabricated by the technique of electrospinning as innovative form-stable PCMs for storage and retrieval of thermal energy.