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A new cluster {Mo3S4[NH2CH2CH(O)CH2NH2]3}(DTP)·(H2O)2·(DMF) (DTP = diethyldithiophosphate) has been synthesized via ligand substitution reaction of Mo3S4(DTP)4(H2O) with an alkaline ligand 1,3-diamino-2-propanol(DAPROH) in a mixed organic solven