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用电弧熔炼锤砧技术，在Ｈｆ－Ｉｒ和Ｚｒ－Ｏｓ二元合金系中制得新的金属玻璃，其成分范围是：Ｈｆ１００－ＸＩｒＸ，Ｘ＝２０～３０ａｔ％；Ｚｒ１００－ＸＯｓＸ，Ｘ＝２０～３０ａｔ％。作者用差示扫描量热计（ＤＳＣ）研究Ｈｆ１００－ＸＩｒＸ和Ｚｒ１００－ＸＯｓＸ（Ｘ＝２０、２５、３０ａｔ％）金属玻璃的结晶行为，测定结晶温度、结晶热和结晶激活能，并用Ｘ射线衍射技术分析Ｈｆ８０Ｉｒ２０和Ｚｒ７５Ｏｓ２５金属玻璃的结晶相转变过程，分别为：Ａ（非晶）→α－Ｈｆ＋Ａ′（非晶）→α－Ｈｆ＋Ｈｆ２Ｉｒ和Ａ（非晶）→Ｏｓ４Ｚｒ１１＋Ａ′（非晶）→Ｏｓ４Ｚｒ１１＋ＯｓＺｒ＋α－Ｚｒ。
A new metallic glass was prepared from Hf-Ir and Zr-Os binary alloy system by the arc melting anvil technique. The composition range of Hf100-XIrX is X = 20 ~ 30at%; Zr100-XOsX, X = 20 ~ 30at%. The authors studied the crystallization behavior of Hf100-XIrX and Zr100-XOsX (X = 20, 25, 30at%) metallic glasses by differential scanning calorimetry (DSC). The crystallization temperature, the heat of crystallization and the activation energy of crystallization were measured and characterized by X-ray diffraction Technical analysis The crystal phase transition of Hf80Ir20 and Zr75Os25 metallic glasses are: A (amorphous) → α-Hf + A ’(amorphous) → α-Hf + Hf2Ir and A (amorphous) → Os4Zr11 + A’ (amorphous) → Os4Zr11 + OsZr + Zr.