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Surface molecularly imprinted polymers (SMIP) was prepared via the reversible addition-fragmentation chain transfer (RAFT) polymerization on the chloromethyl polystyrene resin (CPR) in the presence of the template D-phenylalanine. The structure of SMIP was characterized by FTIR and SEM. The adsorption behavior of D-phenylalanine of SMIP was preliminarily investigated.