【摘 要】
：
W4S4 [S2P (OEt)2]6, Mr= 1974. 94, triclinic, P1, a = 14. 063 (5) , b = 16. 289(4), c= 13. 377(3) A ,α=92. 06 (2), β=95. 24(3), γ= 73. 06(2)°, V= 2919(3)A3,
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W4S4 [S2P (OEt)2]6, Mr= 1974. 94, triclinic, P1, a = 14. 063 (5) , b = 16. 289(4), c= 13. 377(3) A ,α=92. 06 (2), β=95. 24(3), γ= 73. 06(2)°, V= 2919(3)A3,Z=2,DC=2. 18g/cm3, Moka radiation,λ =0. 71069A ,μ = 90. 64cm-1, F(000) = 1764,R=0. 053 and Rw = 0. 069 for 5422 reflections with I≥3σ(I).The title compound is comprised of a cubane-like cluster core [W4S4] in which every W atom is coordinated by six S atoms to form a distorted octahedron.
(4), c = 13. 377 (3) A, α = 0, W = Γ = 73.06 (2) °, V = 2919 (3) A3, Z = 2, DC = 2.18g / cm3, Moka radiation, λ = 0. 71069A, μ = 90. 64cm -1, F (000) = 1764, R = 0. 053 and Rw = 0. 069 for 5422 reflections with I ≥ 3σ (I). The title compound is comprised of a cubane -like cluster core [W4S4] in which every W atom is coordinated by six S atoms to form a distorted octahedron.
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