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Three new silver alkylenediphosphonates,[Ag2(HO3PCH2CH2CH2CH2PO3H)]1,[Ag4(O3PCH2CH2CH2CH2PO3)]2 and [Ag4(O3PCH2CH2CH2PO3)(H2O)]3,have been hydrothermally synthesized and characterized by X-ray single-crystal and powder diffraction, elemental analyses, IR