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The title compound(E)-N1,N4-bis(2,3,4-trimethoxy-6-methylbenzylidene) butane-1,4-diamine(C26H36N2O6,Mr = 472.57) was synthesized and characterized by elemental analysis,IR spectra and single-crystal X-ray diffraction.The crystal belongs to triclinic,space group C2/c with a = 36.102(4),b = 5.6620(11),c = 13.015(2) ,β = 105.491(2)o,V = 2563.7(7) 3,Z = 4,Dc = 1.224 g/cm3,λ = 0.71073 ,μ(MoKα) = 0.087 mm-1,F(000) = 1016,the final R = 0.0456 and wR = 0.1257 for 2255 observed reflections with I > 2σ(I).X-ray diffraction analysis reveals that the molecule adopts an E configuration about the central C=N functional bond.The phenyl rings of two 2,3,4-trimethoxy-6-methylbenzaldehyde groups are parallel by symmetry.The molecules are linked through π-π and C-H…π stacking interactions and C-H…O hydrogen bonding interactions.The title compound possesses moderate antibacterial activity.
The title compound (E) -N1, N4-bis (2,3,4-trimethoxy-6-methylbenzylidene) butane- 1,4- diamine (C26H36N2O6, Mr = 472.57) was synthesized and characterized by elemental analysis, IR spectra and space group C2 / c with a = 36.102 (4), b = 5.6620 (11), c = 13.015 (2) , β = 105.491 (2) o, V = 2563.7 (7) 3, Z = 4, Dc = 1.224 g / cm3, λ = 0.71073 μ, μ (MoKα) = 0.087 mm -1, F (000) = 1016, 0.1257 for 2255 observed reflections with I> 2σ (I). X-ray diffraction analysis reveals that the molecule adopts an E configuration about the central C = N functional bond. The phenyl rings of two 2,3,4-trimethoxy-6- methylbenzaldehyde groups are parallel by symmetry. The molecules are linked through π-π and CH ... π stacking interactions and CH ... O hydrogen bonding interactions. title of title compound possesses moderate antibacterial activity.