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建立了一个手动快速放射化学分离程序以测定 ̄(252)Cf自发裂变产物中的 ̄(114)pd,其主要分离步骤是萃取和沉淀Pd(DMG)_2配合物。分离程序耗时5.5-6min,化学回收率为30%-60%。方法的精密度以单次测量值的相对标准偏差表示,为3.9%。
A manual rapid radiochemical separation procedure was established to determine the (114) pd in ~ (252) Cf spontaneous fission products. The main separation step was the extraction and precipitation of Pd (DMG) 2 complex. Separation procedures take 5.5-6min, chemical recovery rate of 30% -60%. The precision of the method, expressed as the relative standard deviation of a single measurement, was 3.9%.