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We have performed low temperature resistivity p(T) and specific heat C(T) measurements on a superconducting polycrystalline Nb0.75Mg0.25B2 sample.The results indicate that the superconducting transition temperature is ～4.6 K.The zero temperature upper critical field determined from the resistivity and specific heat is 3123 Oe.The electronic coefficient of specific heat γn=4.51 mJ mol-1 K2 and the Debye temperature θn=419 K are obtained by fitting the zero-field specific heat data in the normal state.At low temperatures,the electronic specific heat in the superconducting state follows Ces/γnTc=2.84 exp(-1.21Tc/T).This indicates that the superconducting pairing in Nb0.75Mg0.25 B2 has s-wave symmetry.