Synthesis and Crystal Structure of {4-[2-(9- Hexyl-9H-carbazol-3-yl)vinyl]phenyl} Dimethylamine

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The title compound {4-[2-(9-hexyl-9H-carbazol-3-yl)vinyl]phenyl} dimethylamine has been synthesized by the well known Wittig reaction, and its crystal structure was determined by single-crystal X-ray diffraction analysis. It crystallizes in monoclinic, space group P21/c with a = 47.87(2), b = 10.222(4), c = 9.612(4)(A), β = 92.401(9)°, V = 4699(3)(A)3, Z = 8, C28H32N2, Mr = 396.56, Dc = 1.121 g/cm3, F(000) = 1712 and μ(MoKa) = 0.065 mm-1. The final R and wR are 0.0793 and 0.1983, respectively for 3524 observed reflections with Ⅰ> 2σ(Ⅰ). In the title compound, the bond lengths are normal, and the crystal is stabilized by Van der Waals forces.
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