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The reaction of half-sandwich complex (Cp^ttRh)2Cl2(μ-Cl)2 (1) (Cp^tt= η^5-^1Bu2C5H3) with 1 equiv, of AgSO3CF3 in CH2Cl2 affords tri-μ-chloro dirhodium (2) cation compound, with 2 equiv, of AgSOaCF3 providing di-μ-chloro complex 3. The reaction of 3 with