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采用常温搅拌法合成了2,3,6-三巯基均三嗪(ttcH3)和4-氨基-3,5-二(3-吡啶基)-1,2,4-三唑(3-bpt)与过渡金属镉的配合物[Cd(ttcH2)2(3-bpt)2]·2H2O,对其结构进行了X-射线单晶衍射、红外光谱、元素分析以及热重分析等表征。X-射线单晶衍射分析显示该配合物为单核,属于三斜晶系,空间群P-1。配合物在氢键作用下拓展为3D超分子网络结构。热重分析显示该配合物的骨架稳定性较好。
(TtcH3) and 4-amino-3,5-bis (3-pyridyl) -1,2,4-triazole (3-bpt) Cd (ttcH2) 2 (3-bpt) 2] · 2H2O complexes with transition metal were characterized by X-ray single crystal diffraction, FTIR, elemental analysis and thermogravimetric analysis. X-ray single crystal diffraction analysis showed that the complex was mononuclear and belongs to the triclinic space group P-1. The complex expands to 3D supramolecular network structure under hydrogen bonding. Thermogravimetric analysis showed that the complex has better stability.