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由2-甲氧基-5-芳偶氮基(艹卓)酮与芳胺直接缩合反应制备了一系列新的2-芳胺基-5-芳偶氮基(艹卓)酮化合物(6a-i),用~1H-NMR和元素分析表征了结构。通过差示扫描量热法研究了其热力学性质,并结合分子结构进行了探讨。
A series of novel 2-arylamino-5-azoazone compounds (6a) were prepared by the direct condensation reaction of 2-methoxy-5-azoazoles with aromatic amines -i). The structure was characterized by ~ 1H-NMR and elemental analysis. The thermodynamic properties were studied by differential scanning calorimetry and the molecular structure was also discussed.