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The title compound (C25H20FN5OS) has been synthesized and its crystal structure was determined by X-ray analysis. The crystal belongs to the orthorhombic system, space group Pbca with a = 10.327(4), b = 20.307(7), c = 21.234(9) ? α = 90, β = 90, γ = 90u001f, V = 4453(3) 3, Z = 8, Dc = 1.365 g/cm3, Mr = 457.52, μ = 0.182 mm-1, F(000) = 1904, the final R = 0.0600 and wR = 0.0932 for 3911obsered reflections with I≥2σ(I). In the title compound, the S(1), C(1), C(2), C(3), C(4), C(5), N(1), N(2), N(3), N(4), O(1) and N(5) atoms form a mean planeⅠroughly within the average deviation of 0.0207 ? The dihedral angles between planesⅠandⅡ(C(19)C(20) C(21)C(22)C(23)C(24)),Ⅲ(C(6)C(7)C(8)C(9)C(10)C(11)) and Ⅳ(C(12)C(13)C(14) C(15)C(16)C(17)C(18)F(1)) are 21.40, 84.00 and 75.88u001f, respectively.
The title compound (C25H20FN5OS) has been synthesized and its crystal structure was determined by X-ray analysis. The crystal belongs to the orthorhombic system, space group Pbca with a = 10.327 (4), b = 20.307 (7), c = 21.234 (9) α = 90, β = 90, γ = 90 u001f, V = 4453 (3) 3, Z = 8, Dc = 1.365 g / cm3, Mr = 457.52, μ = 0.182 mm-1, F 000) = 1904, the final R = 0.0600 and wR = 0.0932 for 3911obsered reflections with I≥2σ (I). In the title compound, the S (1), C (1), C (2), C (4), C (4), C (5), N (1), N (2), N (3), N 0.0207? The dihedral angles between planes I and II C (6) C (7) C (8) C (21) C C (18) F (1)) are 21.40, C (10) C (11)) and IV (C (12) C 84.00 and 75.88 u001f, respectively.