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A copper(Ⅰ)-iodide coordination polymer,namely{[Cu3 I3(Tipa)2]·3(DMF)}n(1),was synthesized from tetrahedral Cu4 I4(py)4 precursor and tris(4-(~1H-imidazol-1-yl)phenyl)amine)(Tipa)ligand in N,N-dimethylformamide(DMF)and methanol,and characterized by s