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An extremely facile and rapid solid phase route free of column chromatographic purification for the synthesis of the soluble monodisperse oligo(1, 4-phenyleneethynylene)s up to～60 was presented.
An extremely facile and rapid solid phase route free of column chromatographic purification for the synthesis of the soluble monodisperse oligo (1, 4-phenyleneethynylene) s up to ~ 60% was presented.