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Fe(Ⅱ) complex Fe[HB(pz)3]2(compound 1, pz=pyrazole) and Ni(Ⅱ) complex Ni[HB(pz)3]2(compound 2) have been obtained by the reaction of MCI2(M=Fe and Ni) with NaHB(pz)3 in MeOH. The two complexes(compounds 1 and 2) were characterized by IR, NMR, elemental an