由于某些有机金属化合物很不稳定,制取困难,获得量甚少,因此迫切需要建立相应的快速分析方法,并尽可能利用一份样品测出多种元素含量,以判断化合物的组成或纯度。虽然有机金属化合物(包括原子簇化合物)中碳、氢和金属的同时快速测定法已有报道,但是,某些有机钼(锌)化合物在高温燃烧氧化过程中,能生成挥发性的金属氧化物,并随着载气吹离样品舟,故不能简单地以高温氧化分解和称样品舟中残渣的方法来进行快速同时测定。本文对Gawargious等人建 Since some organometallic compounds are very unstable, difficult to prepare and obtain very little, there is an urgent need to establish a corresponding rapid analytical method and to use as many samples as possible to detect the content of various elements to determine the composition or purity of the compound . Although simultaneous rapid determination of carbon, hydrogen and metals in organometallic compounds, including cluster compounds, has been reported, certain organo-molybdenum (Zn) compounds can generate volatile metal oxides during high temperature combustion and oxidation , And as the carrier gas blows off the sample boat it can not be quickly and simultaneously determined simply by high temperature oxidative decomposition and by weighing the residue in the sample boat. This article was built by Gawargious et al