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A two-dimensional coordination polymer,(NH3+CH2CH2NH3+)(NH2CH2CH2NH3+)2[(VO)4(PO4)4(H2O)].2H2O has been obtained by using hydrothermal synthesis and characterized by elemental analysis,IR spectrum and X-ray single crystal diffraction.The compound crystallized in the monoclinic system,space groupP2(1) /c,a=17.034(4) A,b=10.351(2) A,c=17.536(4)A,β=114.641(4)°,z=4,V=2810.3(11)A3,Dc=2.108g/cm3,F(000)=1784,R1=0.0375,ωR2=0.1047.
2H2O has been obtained by using hydrothermal synthesis and characterized by elemental analysis, IR spectrum and X-ray. A two-dimensional coordination polymer (NH3 + CH2CH2NH3 +) (NH2CH2CH2NH3 +) 2 [(VO) 4 single crystal diffraction. The compound crystallized in the monoclinic system space group P2 (1) /c,a=17.034(4) A, b = 10.351 (2) A, c = 17.536 °, z = 4, V = 2810.3 (11) A3, Dc = 2.108g / cm3, F (000) = 1784, R1 = 0.0375, ωR2 = 0.1047.