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The title compound (C28H19Cl2N) has been synthesized by the reaction of diben- zoylmethane and N-(4-chlorobenzylidene)-4-chlorobenzenamine promoted by low-valent titanium reagent, and characterized by elemental analysis, IR, 1H NMR and X-ray single-crystal diffraction. The crystal belongs to monoclinic, space group P21/c with a = 9.952(2), b = 9.863(2), c = 23.460(6) ?, β = 99.62(2)°, V = 2270.4(9) ?3, Mr = 440.34, Z = 4, Dc = 1.288 g/cm3, μ(MoKα) = 0.301 mm-1, F(000) = 912, the final R = 0.0387 and wR = 0.0793. X-ray analysis reveals that the four phenyl rings in the pyrrole ring are not coplanar.
The title compound (C28H19Cl2N) has been synthesized by the reaction of dibenzylidene and N- (4-chlorobenzylidene) -4-chlorobenzenamine promoted by low-valent titanium reagent, and characterized by elemental analysis, IR, 1H NMR and X-ray The crystal belongs to monoclinic, space group P21 / c with a = 9.952 (2), b = 9.863 (2), c = 23.460 (6) ?,? = 99.62 (2) °, V = 2270.4 (9)? 3, Mr = 440.34, Z = 4, Dc = 1.288 g / cm3, μ (MoKα) = 0.301 mm-1, F (000) = 912, the final R = 0.0387 and wR = ray analysis reveals that the four phenyl rings in the pyrrole ring are not coplanar.