Effect of TiO2 addition on zirconia-mullite composites fabricated by in-situ controlled crystallizat

来源 :中南大学学报(英文版) | 被引量 : 0次 | 上传用户:du_go666
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
Zirconia-mullite composite ceramics were fabricated by in-situ controlled crystallization of Si-Al-Zr-O amorphous bulk.The effects of TiO2 addition on the fabrication of zirconia-mullite composites were investigated.The ultra-fine zirconia-mullite composite ceramics were prepared from the amorphous bulk treated.at 980 ℃ for nucleation and 1 140 ℃ for crystallization.The phase transformation of the ceramics was examined using differential scanning calorimetry (DSC) and X-ray diffractometry (XRD).The microstructural features of the samples were evaluated with scanning electron microscopy (SEM),energy dispersive spectroscopy (EDX) and transmission electron microscopy (TEM).The mechanical properties were also determined using Vickers indentation.The results show that the TiO2 additives with mass fraction of 1%-7% reduce the formation temperature of t-ZrO2 and mullite.When the mass fraction of TiO2 additives is less than 5%,the phases do not change,and most of TiO2 dissolves in ZrO2.When the mass fraction of TiO2 additives is over 5%,the excessive TiO2 forms a new phase,ZrTiO4.Meanwhile,the results also show that TiO2 additives have a great impact on the microstructure and mechanical properties of zirconia-mullite composites.As the TiO2 content increases from 1% to 7% (mass fraction),the grain size and the Vickers hardness of zirconia-mullite composites increase.The composite with 3% (mass fraction) TiO2 additives attains relatively higher fracture toughness.
其他文献
2001年12月20日,国家经济贸易委员会发布2001年第30号公告:《发布职业安全健康管理体系指导意见和职业安全健康管理体系审核规范》(以下简称《指导意见》和《审核规范》)。这标志着我国职业安全
新世纪需要的是创新人才,成为创新人才的关键是创新思维能力的培养,我国著名的教育家陶行知先生说:“处处都是创造之地,天天都是创造之时,人人都是创造之才。”“创新教育”
期刊
本文通过对荣华二采区10
期刊
近日,台湾地区食药署发布消息,通报越南生蚝产品检出肠炎弧菌及沙门菌。这两种菌对消费者有什么样的危害?国内外有何标准要求?怎样防控风险?日前,国家食品药品监督管理总局发
本文通过对荣华二采区10
期刊
记者rn2016年是我国智慧城市建设稳步推进的一年,在您看来,2016年我国智慧城市建设领域有哪些创新性的突破和发展?可以用哪些关键词来表述?rn刘朝晖rn大家好,非常高兴与大家
期刊
告别了欢乐祥和的春节长假,你是否感叹假期走了,肥肉却留下了一堆?春节期间,大家平时的生活和工作节奏都被打乱了,很多人都是晚睡晚起,胡吃海喝,餐桌上还烟酒不离手。回到工
本文介绍了GE 1.5T超导型核磁共振的几例故障,并阐述了查找故障原因以及排除故障的过程.