论文部分内容阅读
醇胺分别与 2 溴 4′ 甲氧基苯乙酮、2 溴 3′ 氯苯丙酮、2 溴 4′ 苄氧基苯基丙酮、2 溴 4′ 苄氧基苯戊酮、6 甲氧基 2 溴乙酰基萘和 6 甲氧基 2 ( 2 溴丙酰基 )萘反应 ,合成相应的 2 芳基 2 吗啉醇 (产率 80 .7%~ 97.5 % )及其盐酸盐 .其结构经1HNMR ,IR ,MS确证
The alcohol amines were reacted with 2 bromo 4’methoxyacetophenone, 2bromo 3’-chloropropiophenone, 2bromo 4’benzyloxyphenylacetone, 2bromo 4’benzyloxyphenylpentanone, 6methoxy2 Bromoacetylnaphthalene and 6methoxy 2 (2bromopropionyl) naphthalene to synthesize the corresponding 2-aryl-2morpholinol (yield 80.7% -97.5%) and its hydrochloride. The structure was confirmed by 1HNMR , IR, MS confirmed