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Two new Ni(Ⅱ) coordination polymers,{[Ni(tbip)(bipy)(H2O)]·0.5H2O}n 1 and [Ni(tbip)(phen)(H2O)]n 2(H2tbip=5-tert-butyl isophthalic acid,bipy=2,2′-bipyridine,phen=1,10-phenanthroline),have been synthesized under hydrothermal conditions and characteriz