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以王水（体积分数为２０％）作移动相，以硅胶球负载的ＴＢＰ作固定相，反相萃取层析使微量Ａｕ（Ⅲ）、Ｔｌ（Ⅲ）与Ｆｅ３＋、Ｃｕ２＋、Ａｇ＋、Ｚｎ２＋、Ｍｎ２＋、Ｈｇ２＋、Ｃｄ２＋、Ｐｂ２＋、Ｓｂ５＋、Ａｓ５＋、Ｇａ３＋、Ｉｎ３＋、Ｐｔ２＋、Ｐｄ２＋等多种离子分离，留于柱上的铊、金分别用ＮａＡｃ溶液（量浓度为１ｍｏｌ／Ｌ）及Ｎａ２ＳＯ３溶液（质量浓度为１０ｇ／Ｌ）洗脱进行连续分离与测定（结晶紫光度法测定铊，孔雀绿光度法测定金），回收率可达９６％以上，方法已应用于地质样品中金、铊的连续分离与测定。
In the presence of aqua regia (20% by volume) as the mobile phase, silica gel loaded TBP was used as the stationary phase. Reverse phase extraction was used to extract the trace amounts of Au (Ⅲ), Tl (Ⅲ) and Fe3 +, Cu2 +, Ag +, Zn2 + , Hg2 +, Cd2 +, Pb2 +, Sb5 +, As5 +, Ga3 +, In3 +, Pt2 + and Pd2 +. The thallium and gold remaining on the column were separated by NaAc solution (concentration 1mol / L) and Na2SO3 solution (10g / L) for continuous separation and determination (determination of the crystal violet spectrophotometry thallium, malachite green spectrophotometric determination of gold), the recovery rate of up to 96%, the method has been applied to geological samples of gold and thallium continuous separation and Determination.