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通过循环伏安电沉积方法在玻碳基底上制备纳米级厚度Ni薄膜(nm-Ni/GC),以CO吸附为探针反应,运用电化学原位傅里叶变换红外(FTIR)反射光谱研究其性能,将所发现的异常红外效应的研究拓宽到铁系Ni金属纳米薄膜.
Nanostructured Ni thin films (nm-Ni / GC) were prepared on glassy carbon substrates by cyclic voltammetry. CO adsorption was used as the probe reaction, and electrochemical in situ Fourier transform infrared (FTIR) Its performance, will discover the abnormal infrared effect of the research to broaden the iron-based Ni metal nano-film.