【摘 要】
：
建立了气相色谱-质谱联用（GC-MS）同时快速检测卷烟主流烟气中5种挥发性有机化合物（1,3-丁二烯,异戊二烯,丙烯腈,苯和甲苯）的分析方法。主流烟气气相物中的挥发性有机化合物被含有
【基金项目】
：
国家自然科学基金项目“新型层状氢氧化物微结构组装体的水相合成、形成机理及应用研究”（20701040）
论文部分内容阅读
建立了气相色谱-质谱联用（GC-MS）同时快速检测卷烟主流烟气中5种挥发性有机化合物（1,3-丁二烯,异戊二烯,丙烯腈,苯和甲苯）的分析方法。主流烟气气相物中的挥发性有机化合物被含有D6-苯内标的冷甲醇吸收,并用GC-MS在选择离子模式下进行分析。方法的最低检出限（LOD）和最低定量限（LOQ）分别为0.01~0.81μg/支和0.04~2.73μg/支,加标回收率为92.3%~98.5%,精密度为1.95%~9.21%。本方法检测限低,重复性和重现性明显优于以前报道的方法。应用此方法考察了38种国内外卷
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