Filter paper-templated preparation of ZnO thin films and examination of their gas-sensing properties

来源 :Particuology | 被引量 : 0次 | 上传用户:ysgmxh
下载到本地 , 更方便阅读
声明 : 本文档内容版权归属内容提供方 , 如果您对本文有版权争议 , 可与客服联系进行内容授权或下架
论文部分内容阅读
ZnO thin films prepared by using quantitative filter paper as a template and Zn(CH3CO2) 2·2H2O ethanol precursor solution were characterized by scanning electron microscopy(SEM) and X-ray diffraction(XRD) . The effects of sample calcination temperature,precursor concentration and filter paper types were studied,and the growth process was investigated by infra-red(IR) spectroscopy and thermogravimetric analysis/differential thermal analysis(TGA/DTA) . The results show that samples soaked in a 1.5 mol/L Zn(CH3CO2) 2·2H2O ethanol solution and calcined at 600 °C yield ZnO films of uniform particle size,approx-imately 30,40 and 50 nm,for fast-,medium-and slow-speed filter papers,respectively. The formaldehyde gas sensing properties of the ZnO nanoparticles were tested,showing that the material prepared from fast-speed filter paper has a higher response to 120-205 ppm formaldehyde at 400 °C than that prepared from medium-or slow-speed paper,which depends on the particle size. ZnO thin films prepared by using quantitative filter paper as a template and Zn (CH3CO2) 2.2H2O ethanol precursor solution were characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The effects of sample calcination temperature, precursor concentration and filter paper types were studied, and the growth process was investigated by infra-red (IR) spectroscopy and thermogravimetric analysis / differential thermal analysis (TGA / DTA). The results show that samples soaked in a 1.5 mol / L Zn 2 · 2H 2 O ethanol solution and calcined at 600 ° C yield ZnO films of uniform particle size, approx-imately 30, 40 and 50 nm for fast-, medium-and slow-speed filter papers, respectively. The formaldehyde gas sensing properties of the ZnO nanoparticles were tested, showing that the material prepared from fast-speed filter paper has a higher response to 120-205 ppm formaldehyde at 400 ° C than that prepared from medium-or slow-speed paper, which depends on the particle size.
其他文献
课堂教学中及时评价的“有效性”研究,不仅有利于提高课堂教学效率,更有利于促进学生潜能、个性和创造性的发挥,对教师自身的发展都有积极的意义。课堂评价的“有效性”势在
通过玻璃介质层的硅片直接键合法形成SOI结构=[刊,俄]1994,23(6).-55~60在集成电路工艺中,采用SOI结构可以大大减小寄生耦合,提高击穿电压,降低所需功率,提高集成密度,加快电路工作速度,提高工作频率和抗辐射加
珍奥集团股份有限公司成立于1996年5月,2003年7月成立珍奥集团。珍奥集团是以珍奥集团股份有限公司为母公司,以大连珍奥药业有限公司、福建珍奥核酸有限公司、上海珍奥企玛
An orthogonal method was used to evaluate the effects of Ga, Al, Ag, and Ce multi-additions on the wetting characteristics of Sn-9Zn lead-free solders by wettin
近年来,西安有一批年轻、有才华的演员涌上舞台,如蓓蕾初绽,竞放芬香,颇受观众赞赏。但我则于赞赏之余,尚感不足。这些青年演员除了在全面的艺术修养和舞台实践经验等方面尚
SiGe技术专题文摘WD95501高性能发射极向上/向下硅-锗异质结晶体管=Highperformanceemitter-up/downSiGeHBT'S[刊,英]/Burghartz,J.N.…∥IEEEElec.Dev,Lett.-1994,15... SiGe Technology Digest WD95501 High Performance Emitter Up / Down Silicon-Ge Heterojunction Transis
记者余春瑜北京报道4月21日,在第十届北京国际汽车展览会上,德国曼公司为其荣膺2008年度卡车称号的明星车型TGX、TGS举行了新车揭幕仪式。这是TGX和TGS在中国乃至亚洲的首次
注册登记一、申请机动车注册登记,应当交验机动车.并提交以下证明、凭证:1、《机动车注册登记/转入申请表》;2、机动车所有人的身份证明和复印件; Registration First, the
6月17日,惠普在国内隆重发布了“动成长企业”(Adaptive Enterprise)战略,并在此战略下专为国内客户定制十大解决方案,分三阶段帮助他们实现“动成长企业”。惠普整合并后,
许步荣同志,现任天津市滨海监狱党委书记、监狱长。参加工作32年来,许步荣同志曾担任副大队长、大队长、副监狱长、副政委、政委、监狱长等职,在历任岗位上都有出色的业绩。