以臭氧为引发剂对SE-33、SE-54及OV-1等非极性固定液弹性石英毛细管柱进行交联。用臭氧法制得的交联弹性毛细管柱具有高效、内壁惰性、热稳定性好及耐溶剂冲洗等优点,这些柱子用于松油、酒及植物中残留烃三种样品的分离,均获得较好的结果。臭氧交联方法简单、适于一般实验室采用。 Using ozone as the initiator, SE-33, SE-54, OV-1 and other non-polar fixed liquid flexible silica capillary column cross-linked. The cross-linked elastic capillary column made by the ozone method has the advantages of high efficiency, inertness of the inner wall, good thermal stability and solvent washing resistance, etc. These columns are used for the separation of three kinds of samples of residual hydrocarbons in pine oil, wine and plants, the result of. Ozone crosslinking method is simple, suitable for general laboratory use.