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在LichrosorbRP-18色谱往上采用流动相甲醇-水-三乙胺(50:50:0.1,pH3.0)、检测波长295nm,在20~100μg/ml范围内,峰面积(A)与对照品浓度(C)呈良好的线性关系,日内、日间RSD分别为0.97%和1.21%,平均回收率为98.98±0.97%,结果满意。
The mobile phase of methanol-water-triethylamine (50:50: 0.1, pH 3.0) was used in the Lichrosorb RP-18 chromatography. The detection wavelength was 295 nm. The peak area (A) was in the range of 20-100 μg / The concentration of reference substance (C) showed a good linear relationship. The intra-day and inter-day RSD were 0.97% and 1.21%, respectively. The average recovery was 98.98 ± 0.97%. The results were satisfactory.